ČSN EN ISO 18363-3

Animal and vegetable fats and oils - Determination of fattyacid- bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 3: Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol

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Detail information

Designation: ČSN EN ISO 18363-3

Publication date: 01/01/2025

Pages: 32

Country: Czech technical standard

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Anotation

This document specifies a procedure for the simultaneous determination of 2-MCPD esters (bound 2 MCPD), 3-MCPD esters (bound 3-MCPD) and glycidyl esters (bound glycidol) in a single assay, based on acid catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC/MS analysis.
This document is applicable to solid and liquid fats and oils. For all three analytes the limit of quantification (LOQ) is 0,1 mg/kg and the limit of detection (LOD) is 0,03 mg/kg

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